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961 minutes (title compound), 2. 313 minutes (urea impurity). Example 8 4-Chloro-6-cyclopropyl-2-(2-trifluoromethyl-phenyl)-pyrimidine: 6-Cyclopropyl-2- (2-trifluoromethyl-phenyl)-3H-pyrimidin-4-one (12. 0 g, 42. 8 mmol) in phosphorous oxychloride (40 mL, 428 mmol) was heated at 75-80¬C for 1 hour.

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GilbertP.Burkholder, J. (2006).]