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5-15 minutes (at the very end of the trial). This procedure has been previously found to represent the animal's 'performance' as displayed throughout the entire trial. Trial LI (second trial): [00138] On day 4 rats are placed again into the cylinder, this time for 5 minutes. Immobility-time is manually recorded throughout the entire trial. fiviani Compound treatments were suspended in 0.

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313 minutes (urea impurity). Example 8 4-Chloro-6-cyclopropyl-2-(2-trifluoromethyl-phenyl)-pyrimidine: 6-Cyclopropyl-2- (2-trifluoromethyl-phenyl)-3H-pyrimidin-4-one (12. 0 g, 42. 8 mmol) in phosphorous oxychloride (40 mL, 428 mmol) was heated at 75-80¬C for 1 hour.

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